- 作 者：CSABA HORVATH
- 出 版 社：ACADEMIC PRESS
- 出版年份：2222
- ISBN：0123122023
- 标注页数：341 页
- PDF页数：351 页
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LIST OF CONTRIBUTORS 7
CONSPECTUS 9
PREFACE 11
CONTENTS OF VOLUME 1 13
Optimization in Liquid Chromatography Georges Guiochon 1
Ⅰ．Introduction 1
Ⅱ．Resolution and Efficiency 2
Ⅲ．AnalysiS Time,Flowrate, and Pressure 6
Ⅳ．Flow Velocity and Column Efficiency 7
Ⅴ．What to Optimize in Liquid Chromatography 15
Ⅵ．Equations Used for Optimization 17
Ⅶ．WayS to Achieve 5000 Plates in 5 Minutes 19
Ⅷ．Column Performance at Minimum Inlet Pressure 29
Ⅸ．Critical Minimum Pressure 33
Ⅹ．Achievement of Fastest Analyses 35
Ⅺ．Practical Considerations 39
Ⅻ．Equipment Specifications 43
ⅩⅢ．Conclusions 52
References 54
Liquid Chromatography on Silica and Alumina as Stationary Phases Heinz Engelhardt and Helmut ElgassⅠ．Introduction 57
Ⅱ．Stationary Phases 60
Ⅲ．Role of the Eluent 70
Ⅳ．Effect of Sample Structure on Retention 90
Ⅴ．Anisocratic Analysis 92
Ⅵ Theory of Adsorption Chromatography 101
Ⅶ．Selected Applications 104
Ⅷ．Prospects 106
References 108
Reversed-Phase Chromatography Wayne R．Melander and Csaba HorváthⅠ．Introduction 114
Ⅱ．The Stationary Phase 123
Ⅲ．The Mobile Phase 165
Ⅳ．Effect of Temperature 192
Ⅴ．Theory of Reversed-Phase Chromatography 201
Ⅵ．Modulation of Selectivity by Secondary Equilibria 229
Ⅶ．Physicochemical Measurements 266
Ⅷ．Selected Analytical Applications 279
Notation 299
References 303
Index 321
Erratum 341